Handbook of Preparative Inorganic Chemistry Vol 2 2d ed - George Brauer.pdf - Inorganic Chemistry - ziolek6661

PREPARED IN COLLABORATION WIT H

M . Baudler, Cologn e

H . J . Becher, Stuttgar t

E. Donges, Gersthofe n

P. Ehrlich, Giesse n

F. Feher, Cologne

O . Glemser, Gottinge n

H . Grube, Hanau

B . Grainer, Wiesbade n

R . Klement, Munic h

W . Kwasnik, Leverkusen

H . Lux, Munich

W . Rudorff, Tubinge n

H . Sauer, Hofhefm/Ts .

P . W . Schenk, Berlin

M . Schmeisser, Aachen

R . Scholder, Karlsruh e

F . Hein, Jena

S . Herzog, Greifswald

F . Seel, Stuttgart

F . Wagenknecht, Sprend -

lingen/Offenbach am Mai n

U . Hofmann, Heidelber g

G. Jander, Berlin

R . Juza, Kiel

R . Wagner, Stuttgart

H . v . Wartenberg, Gottinge n

K. Wetzel, Leipzi g

HANDBOOK O F

INORGANI C

CHEMISTR Y

VOLUME 2 • SECOND EDITIO N

Edited by GEORG BRAUE R

PROFESSOR OF INORGANIC CHEMISTR Y

UNIVERSITY OF FREIBURG

TRANSLATED BY SCRIPTA TECHNICA, INC .

TRANSLATION EDITO R

PAUL G . STECHE R

MERCK SHARP & DOHME RESEARCH LABORATORIE S

1965

ACADEMIC PRESS • New York • London

PREPARATIV E

• ••

ALL RIGHTS RESERVE D

NO PART OF THIS BOOK MAY BE REPRODUCED IN ANY FOR M

BY PHOTOSTAT, MICROFILM, OR ANY OTHER MEANS ,

WITHOUT WRITTEN PERMISSION FROM THE PUBLISHER S

ACADEMIC PRESS INC .

111 FIFTH AVENU E

New Yom, NEW Yor k 10003

United-Kingdom Edition

Published by

ACADEMIC PRESS INC . (LONDON) LTD .

BERKELEY SQUARE HOUSE, LONDON W . 1

Library of Congress Catalog Card Number : 63-14307

Translated from the Germa n

HANDBUCH DER PRAPARATIVEN ANORGANISCHEN CHEMI E

BD . 2, pp . 885-1611, 1962

Published by

FERDINAND ENKE VERLAG, STUTTGAR T

PRINTED IN THE UNITED

STATES OF AMERICA

Translation Editor's Preface

The English version of Volume II of Brauer's "Handbook" follows

the path of the very well received translation of Volume I . Again,

some of the material and particularly the bibliography has been

corrected and brought up to date . The nomenclature has been re-

vised where necessary, with the Stock and the Stock-Werner system s

(the practice of using Roman numerals to define oxidation states of

atoms) adopted as much as possible . This conforms with curren t

I. U . P. A . C . and Chemical Abstracts practice [for details of this ,

see Robert C . Brasted, J. Chem. Education 35, 136 (1948)] . The

references to laboratory equipment and techn iques reflect current

U .S . usage, but useful European methods have been retained .

It is hoped that this volume will be as well received as the pre -

ceding one . Comments from users are invited to help improve

future editions .

Paul G . Steohe r

Rahway, N . J.

May 1965

Contents

TRANSLATION EDITOR'S PREFACE

Part II (continued)

Elements and Compound s

SECTION 19 .

COPPER, SILVER, GOLD

100 3

Copper (Pure Metal)

100 3

Colloidal Copper

100 3

Copper Hydride CuH

100 4

Copper (I) Chloride CuCl

1005

Copper (I) Bromide CuBr

100 6

Copper (I) Iodide CuI

100 7

Copper (II) Chloride CuC1 2

100 8

Copper (II) Bromide CuBr 2

1009

Copper Oxychloride CuC1 2 • Cu(OH) 2

101 0

Copper (I) Oxide Cu 2 0

101 1

Copper (II) Oxide CuO

101 2

Copper (II) Hydroxide Cu(OH) 2

101 3

Potassium Cuprate (III) KCuO 2

101 4

Schweizer's Reagent

101 6

Copper (I) Sulfide Cu 2 S

101 6

Copper (II) Sulfide CuS

101 7

Copper (I) Selenide Cu 2 Se

101 9

Copper (I) Telluride CugTe

1019

• • • • • • • • • • • • • • • • • • • . 1020

Tetraamminecopper (II) Sulfate (Cu(NH3 ) 4)SO 4 • H 2O

102 1

Copper (I) Nitride Cu3 N

102 1

Copper (II) Azide Cu(N 3 ) 2

102 2

Copper Phosphide Cu3 P

102 3

Copper Diphosphide CuP 2

102 4

Carbonates CuCO3 • Cu(OH) 2 (Green

Cupric Carbonate)

Copper

1024

2 CuCO 3 • Cu(OH) 2 (Blue Cupric Carbonate)

102 5

Copper (I) Acetylide Cu 2 C 2 • H 2 O

102 6

Paris Green (Copper Acetoarsenite)

102 7

Fehling's Solution

102 7

Very Pure Silver

102 8

Silver Powder

1029

Silver from Residues

102 9

Silver Mirrors

103 1

Colloidal Silver

1034

Silver Iodide AgI

1035

Silver Chlorate AgC1O3

1037

vi i

Copper (I) Sulfate CuSO 4

Basic

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