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Multidimensional Chromatography
Edited by Luigi Mondello, Alastair C. Lewis and Keith D. Bartle
Copyright © 2002 John Wiley & Sons Ltd
ISBNs: 0-471-98869-3 (Hardback); 0-470-84577-5 (Electronic)
Multidimensional Chromatography
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Multidimensional
Chromatography
LUIGI MONDELLO
Dipartimento Farmaco-chimico, Università degli Studi di Messina, Italy
ALASTAIR C. LEWIS
School of Chemistry and School of the Environment, University of Leeds, UK
KEITH D. BARTLE
School of Chemistry, University of Leeds, UK
JOHN WILEY & SONS, LTD
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Copyright © 2002 by John Wiley & Sons Ltd,
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Library of Congress Cataloging-in-Publication Data
Mondello Luigi.
Multidimensional chromatography / Luigi Mondello, Alastair C. Lewis, Keith D. Bartle.
p. cm
Includes bibliographical references and index.
ISBN 0-471-98869-3
1. Chromatographic analysis. I. Lewis, Alastair C. II. Bartle, Keith D. III. Title.
QD79.C4 M65 2001
543 .089—dc21
2001046684
British Library Cataloguing in Publication Data
A catalogue record for this book is available from the British Library
ISBN 0 471 98869 3
Typeset in 10/12pt Times by Thomson Press (India) Limited, New Delhi
Printed and bound in Great Britain by Biddles Ltd, Guildford and King’s Lynn.
This book is printed on acid-free paper responsibly manufactured from sustainable forestry,
in which at least two trees are planted for each one used for paper production.
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CONTENTS
List of Contributors
xi
Preface
xiii
PART 1: GENERAL
1
1 Introduction
3
K.D. Bartle
1.1 Preamble
3
1.2 Packed Capillary Column and Unified Chromatography
4
1.3 Resolving Power of Chromatographic Systems
6
1.5 The Origins of Multidimensional Chromatography
12
Acknowledgements
13
References
13
2 Coupled High Performance Liquid Chromatography with High
Resolution Gas Chromatography
17
L. Mondello
2.1 Introduction
17
2.2 Transfer Techniques
18
2.3 Vaporization with Hot Injectors
25
2.4 Transfer of Water-Containing Solvent Mixtures
28
2.5 Indirect Introduction of Water
31
2.6 Conclusions
38
References
42
3 Multidimensional High Resolution Gas Chromatography
47
A. C. Lewis
3.1 Introduction
47
3.2 Practical Two-Dimensional Gas Chromatography
48
3.3 Practical Examples of Two-Dimensional Chromatography
57
3.4 Conclusions
72
References
72
4 Orthogonal GC – GC
77
P. J. Marriott
4.1 Introduction to Multidimensional Gas Chromatography
77
4.2 Introduction to GC
GC Separation
80
1.4 Two-Dimensional Separations
9
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