Multidimensional Chromatography (Luigi Mondello, Alastair C. Lewis & Keith D. Bartle).pdf

Multidimensional Chromatography

Edited by Luigi Mondello, Alastair C. Lewis and Keith D. Bartle

ISBNs: 0-471-98869-3 (Hardback); 0-470-84577-5 (Electronic)

Multidimensional Chromatography

Multidimensional

Chromatography

LUIGI MONDELLO

Dipartimento Farmaco-chimico, Università degli Studi di Messina, Italy

ALASTAIR C. LEWIS

School of Chemistry and School of the Environment, University of Leeds, UK

KEITH D. BARTLE

School of Chemistry, University of Leeds, UK

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Library of Congress Cataloging-in-Publication Data

Mondello Luigi.

Multidimensional chromatography / Luigi Mondello, Alastair C. Lewis, Keith D. Bartle.

p. cm

Includes bibliographical references and index.

ISBN 0-471-98869-3

1. Chromatographic analysis. I. Lewis, Alastair C. II. Bartle, Keith D. III. Title.

QD79.C4 M65 2001

543 .089—dc21

2001046684

British Library Cataloguing in Publication Data

A catalogue record for this book is available from the British Library

ISBN 0 471 98869 3

Typeset in 10/12pt Times by Thomson Press (India) Limited, New Delhi

Printed and bound in Great Britain by Biddles Ltd, Guildford and King’s Lynn.

This book is printed on acid-free paper responsibly manufactured from sustainable forestry,

in which at least two trees are planted for each one used for paper production.

CONTENTS

List of Contributors

Preface

xiii

PART 1: GENERAL

1 Introduction

K.D. Bartle

1.1 Preamble

1.2 Packed Capillary Column and Uniﬁed Chromatography

1.3 Resolving Power of Chromatographic Systems

1.5 The Origins of Multidimensional Chromatography

Acknowledgements

References

2 Coupled High Performance Liquid Chromatography with High

Resolution Gas Chromatography

L. Mondello

2.1 Introduction

2.2 Transfer Techniques

2.3 Vaporization with Hot Injectors

2.4 Transfer of Water-Containing Solvent Mixtures

2.5 Indirect Introduction of Water

2.6 Conclusions

References

3 Multidimensional High Resolution Gas Chromatography

A. C. Lewis

3.1 Introduction

3.2 Practical Two-Dimensional Gas Chromatography

3.3 Practical Examples of Two-Dimensional Chromatography

3.4 Conclusions

References

4 Orthogonal GC – GC

P. J. Marriott

4.1 Introduction to Multidimensional Gas Chromatography

4.2 Introduction to GC

GC Separation

1.4 Two-Dimensional Separations

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